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X-ray single crystal diffractometry

Single Crystal Diffractometer Stoe IPDS II

2-circle goniometer (ω-range: 180°, Φ-range: unlimited); imaging plate detector with an active scan diameter of 340mm (2θ-max: 77°); graphite monochromatized Mo-K_α radiation; X-ray fibre optic for intensity enhancement; video CCD-camera for centring and determination of the size/shape of the crystal; computer controlled HEATSTREAM high temperature attachment for the temperature range up to 1100K (in-house development in collaboration with Stoe&Cie., J. Appl. Cryst. (2009) 42, 140-142)

Single Crystal Diffractometer Oxford Diffraction Gemini R Ultra

4-circle kappa-goniometer; 135mm Ruby CCD detector; dual wavelength system: Mo-K_α radiation (graphite monochromator, mono-capillary collimator) & Cu-Ka radiation (multi-layer optics, 300 micron beam size); video CCD-camera for centring and determination of the size/shape of the crystal; Oxford Cryosystems 700 series Cryostream Plus low temperature attachment for the temperature range between 80 and 500K